| Physico- chemical tests |
|
|
|
| Titratable acidity |
БДС 6996 |
12.99 |
+ |
| Total ash |
БДС 7646 |
6.75 |
+ |
| Protein |
БДС 14431, БДС 15438 |
23.01 |
+ |
| рН |
БДС 11688 |
4.09 |
+ |
| Nitrates |
БДС EN 12014-2 |
16.87 |
+ |
| Chlorides |
БДС 7168 |
8.59 |
+ |
| Moisture/ dry matter content |
БДС 15437 |
6.75 |
+ |
| Free fat |
БДС 6997 |
12.14 |
+ |
| Fat |
БДС 8549 |
12.14 |
+ |
| Sugars (total) |
БДС 7169 |
15.34 |
+ |
| Sugars / lactose, glucose, sucrose, fructose |
ILM33HPLC |
15.34 |
+ |
| Soluble substances |
БДС 17257 |
5.39 |
+ |
| Patulin |
БДС EN 14177 |
67.49 |
+ |
| Saturated/ Unsaturated fatty acids |
ILM63GC-FID |
52.15 |
+ |
| Trans fatty acid isomers |
ILM63GC-FID |
120.15 |
+ |
| Sorbic acid / Potassium sorbate |
ILM40HPLC |
23.26 |
+ |
| Benzoic acid / Sodium benzoate |
ILM40 HPLC |
23.26 |
+ |
| Carbohydrates |
ILM22 |
13.5 |
+ |
| Dietary fibre (fibres)-total, soluble and insoluble |
AOAC 985.29, AOAC 991.43 |
80.99 |
+ |
| Energy value |
Regulation (EU) No 1169/2011 Annex XIV (Calculation using conversion factors) |
– |
+ |
| Organoleptic testing |
БДС 1035 |
4.09 |
+ |
| Water activity |
БДС ISO 18787 |
10.12 |
+ |
| Hydroxymethylfurfural (HMF) |
ВЛМ 69HPLC |
16.87 |
+ |
| Total sulfur dioxide |
БДС 11709 т.1.2 |
19.68 |
+ |
| Cyclamate |
БДС EN 12857 |
26.08 |
– |
| Saccharine |
БДС EN 12856 |
26.08 |
– |
| Aspartame |
БДС EN 12856 |
26.08 |
– |
| Acesulfame K |
БДС EN 12856 |
26.08 |
– |
| Drained weight in% of net mass |
БДС 7181 |
2.71 |
– |
| Nitrogen by the Keldal method |
ILM71 Kjeldahl |
23.01 |
– |
| Starch |
Regulation (EC) № 118/2010 Annex I |
66.47 |
+ |
| Element structure |
|
|
|
| Mineralization of 1 sample for testing of elemental composition |
Microwave decomposition |
13.50 |
+ |
| Arsenic / As |
ILM75 ICP-OES |
19.38 |
+ |
| Mercury / Hg |
ILM75 ICP-OES |
19.38 |
+ |
| Nickel / Ni |
ILM75 ICP-OES |
11.91 |
+ |
| Sodium / Na |
ILM75 ICP-OES |
11.91 |
+ |
| Lead / Pb |
ILM75 ICP-OES |
11.91 |
+ |
| Cadmium / Cd |
ILM75 ICP-OES |
11.91 |
+ |
| Calcium / Ca |
ILM75 ICP-OES |
11.91 |
+ |
| Magnesium / Mg |
ILM75 ICP-OES |
11.91 |
+ |
| Chromium / Cr |
ILM75 ICP-OES |
11.91 |
+ |
| Zinc / Zn |
ILM75 ICP-OES |
11.91 |
+ |
| Copper / Cu |
ILM75 ICP-OES |
11.91 |
+ |
| Potassium / K |
ILM75 ICP-OES |
11.91 |
+ |
| Antimony/Sb |
ILM75 ICP-OES |
19.38 |
+ |
| Selenium / Se |
ILM75 ICP-OES |
19.38 |
+ |
| Tin /Sn |
ILM75 ICP-OES |
19.38 |
+ |
| Manganese /Mn |
ILM75 ICP-OES |
11.91 |
+ |
| Iron / Fe |
ILM75 ICP-OES |
11.91 |
+ |
| Phosphorus / P |
ILM75 ICP-OES |
11.91 |
+ |
| Aluminum / Al |
ILM75 ICP-OES |
11.91 |
+ |
| Microbiological tests |
|
|
|
| Total plate count |
БДС EN ISO 4833-1/A1, БДС EN ISO 4833-2/A1, БДС 1035, БДС 6916 |
11.25 |
+ |
| Listeria monocytogenes / Listeria spp. |
БДС EN ISO 11290-1, БДС EN ISO 11290-2 |
20.25 |
+ |
| Salmonella spp. |
БДС EN ISO 6579-1/A1 |
19.43 |
+ |
| Enterobacteriaceae |
БДС EN ISO 21528-2, БДС EN ISO 21528-1 |
9.71 |
+ |
| Escherichia coli |
БДС ISO 16649-1, БДС ISO 16649-2, БДС EN ISO 16649-3 |
10.23 |
+ |
| Coagulase-positive staphylococci/Staphylococcus aureus |
БДС EN ISO 6888-1, БДС EN ISO 6888-2, БДС EN ISO 6888-3+AC |
11.76 |
+ |
| Moulds and yeasts |
БДС ISO 21527-1, БДС ISO 21527-2, БДС 1035, БДС 6916 |
7.67 |
+ |
| Coliforms |
ISO 4832, ISO 4831 |
12.99 |
+ |
| Clostridium perfringens |
БДС EN ISO 7937 |
16.21 |
+ |
| Sulphite reducing clostridia |
ISO 15213 |
16.21 |
+ |
| Bacillus cereus |
БДС EN ISO 7932 |
9.46 |
+ |
| Mesophilic anaerobic microorganisms |
БДС 1035, БДС 6916 |
10.79 |
+ |
| Thermophilic aerobes and facultative anaerobes |
БДС 1035, БДС 6916 |
10.23 |
+ |
| Thermophilic anaerobic microorganisms |
БДС 1035, БДС 6916 |
10.79 |
+ |
| Pseudomonas aeruginosa |
БДС EN ISO 13720 |
12.14 |
– |
| Bacillus spp. |
БДС EN 15784 |
10.12 |
– |
| Mesophilic lactic acid bacteria |
БДС ISO 15214 |
13.5 |
– |
