| Physico- chemical tests |
|
|
|
| Moisture/ Dry matter content |
БДС EN ISO 712-1 |
6.75 |
+ |
| Protein / Crude protein |
БДС 13490 |
23.01 |
+ |
| Crude fat / Fat |
БДС 11374 |
12.14 |
+ |
| Total ash / Crude ash |
БДС EN ISO 2171 |
6.75 |
+ |
| Ash, insoluble in hydrochloric acid |
БДС 754 |
6.75 |
+ |
| Acidity |
БДС 754 |
12.99 |
+ |
| Chlorides |
БДС 11374 |
8.59 |
+ |
| Crude fibres |
БДС 11374 |
23.62 |
+ |
| Sugars/lactose, glucose, sucrose, fructose |
ILM33HPLC |
15.34 |
+ |
| Wet gluten |
БДС EN ISO 21415-1 |
8.59 |
+ |
| Allocation of gluten |
БДС 754 |
6.75 |
+ |
| Aflatoxin В1 and the sum of aflatoxins В1, В2, G1 and G2 |
БДС EN ISO 16050 |
70.56 |
+ |
| Ochratoxin A |
ISO 15141 |
70.56 |
+ |
| Zearalenone |
БДС EN 15792 |
70.56 |
+ |
| Deoxynivalenol |
БДС EN 15791 |
70.56 |
+ |
| Saturated/ Unsaturated fatty acids |
ILM63GC-FID |
52.15 |
+ |
| Trans fatty acid isomers |
ILM63GC-FID |
120.15 |
+ |
| Sorbic acid/ Potassium sorbate |
ILM40HPLC |
23.26 |
+ |
| Benzoic acid/Sodium benzoate |
ILM40HPLC |
23.26 |
+ |
| Carbohydrates |
ILM22 |
13.5 |
+ |
| Dietary fibre (fibres)-total, soluble and insoluble |
AOAC 985.29, AOAC 991.43 |
80.99 |
+ |
| Energy value |
Regulation (EU) No 1169/2011 Annex XIV (Calculation using conversion factors) |
– |
+ |
| Water activity |
БДС ISO 18787 |
10.12 |
+ |
| Impurities |
БДС ISO 605 |
2.68 |
– |
| Falling number |
БДС EN ISO 3093 |
24.54 |
– |
| Acrylamide |
ВЛМ 79LC-MS/MS |
70.3 |
– |
| Polyols |
ВЛМ 33HPLC |
15.34 |
– |
| Element structure |
|
|
|
| Mineralization of 1 sample for testing of elemental composition |
Microwave decomposition |
13.5 |
+ |
| Arsenic / As |
ILM75 ICP-OES |
19.38 |
+ |
| Mercury / Hg |
ILM75 ICP-OES |
19.38 |
+ |
| Nickel / Ni |
ILM75 ICP-OES |
11.91 |
+ |
| Sodium / Na |
ILM75 ICP-OES |
11.91 |
+ |
| Lead / Pb |
ILM75 ICP-OES |
11.91 |
+ |
| Cadmium / Cd |
ILM75 ICP-OES |
11.91 |
+ |
| Calcium / Ca |
ILM75 ICP-OES |
11.91 |
+ |
| Magnesium / Mg |
ILM75 ICP-OES |
11.91 |
+ |
| Chromium / Cr |
ILM75 ICP-OES |
11.91 |
+ |
| Zinc / Zn |
ILM75 ICP-OES |
11.91 |
+ |
| Copper / Cu |
ILM75 ICP-OES |
11.91 |
+ |
| Potassium / K |
ILM75 ICP-OES |
11.91 |
+ |
| Tin /Sn |
ILM75 ICP-OES |
19.38 |
+ |
| Iron / Fe |
ILM75 ICP-OES |
11.91 |
+ |
| Phosphorus / P |
ILM75 ICP-OES |
11.91 |
+ |
| Antimony/Sb |
ILM75 ICP-OES |
19.38 |
– |
| Selenium / Se |
ILM75 ICP-OES |
19.38 |
– |
| Manganese /Mn |
ILM75 ICP-OES |
11.91 |
– |
| Aluminum / Al |
ILM75 ICP-OES |
11.91 |
– |
| Microbiological tests |
|
|
|
| Total plate count |
БДС EN ISO 4833-1/A1, БДС EN ISO 4833-2/A1 |
6.75 |
+ |
| Listeria monocytogenes / Listeria spp |
БДС EN ISO 11290-1, БДС EN ISO 11290-2 |
20.25 |
+ |
| Salmonella spp. |
БДС EN ISO 6579-1/A1 |
19.43 |
+ |
| Enterobacteriaceae |
БДС EN ISO 21528-2, БДС EN ISO 21528-1 |
9.71 |
+ |
| Escherichia coli |
БДС ISO 16649-1, БДС ISO 16649-2, БДС EN ISO 16649-3 |
10.23 |
+ |
| Coagulase-positive staphylococci /Staphylococcus aureus |
БДС EN ISO 6888-1, БДС EN ISO 6888-2, БДС EN ISO 6888-3+AC |
11.76 |
+ |
| Moulds and yeasts |
БДС ISO 21527-1, БДС ISO 21527-2 |
7.67 |
+ |
| Coliforms |
ISO 4832, ISO 4831 |
12.99 |
+ |
| Clostridium perfringens |
ISO 15213-2 |
16.21 |
+ |
| Sulphite reducing clostridia |
ISO 15213-1 |
16.21 |
+ |
| Bacillus cereus |
БДС EN ISO 7932 |
9.46 |
+ |
| Bacillus subtilis / mesentericus |
БДС 15090 |
10.12 |
+ |
| Pseudomonas aeruginosa |
БДС EN ISO 13720 |
12.14 |
– |
| Bacillus spp. |
БДС EN 15784 |
10.12 |
– |
| Mesophilic lactic acid bacteria |
БДС ISO 15214 |
13.5 |
– |
